Beilstein J. Org. Chem.2009,5, No. 72, doi:10.3762/bjoc.5.72
substrates, namely 15.3 ± 3.4 MPa to enamel and 18.5 ± 2.3 MPa to dentin.
Keywords: adhesion to enamel and dentin; hydrolytic stability; N-alkyl-N-(phosphonoethyl) substituted (meth)acrylamides; polymerization enthalpy; REMinvestigation; Introduction
In the past decades dental adhesives have been employed
the adhesive was cured on tooth three times for 20 s.
At last the prepared teeth were stored in water at 37 °C for 2 h before measured.
REMinvestigation was done according to the following procedure: Tooth samples were polished with Nupro (Dentsply), etched with Conditioner 36 (Dentsply) or ethanol
PDF
Graphical Abstract
Scheme 1:
Synthesis of novel N-alkyl-N-(ethyl phosphonate) (meth)acrylamides 3. For 2a, 2b, 3a, 3b: R1 = H, x...